WEKO3
インデックスリンク
アイテム
蛍光誘導体化試薬4-(5，6-ジメトキシ-2-フタルイミジニル)-2-メトキシフェニルスルホニルクロリドを用いる転移性骨腫瘍患者の尿中N-エチルグリシンのHPLCによる定量(発表論文抄録(2008))
https://fukuyama-u.repo.nii.ac.jp/records/8569
https://fukuyama-u.repo.nii.ac.jp/records/8569ed3b56c9-a5ba-40bb-8a21-37cff4f4dfb8
| 名前 / ファイル | ライセンス | アクション |
|---|---|---|
Determination of N-Ethylglycine in Urine of Cancer Patients with Metastatic Bone Disease by HPLC Using 4-(5,6-Dimethoxy-2-phthalimidinyl)-2-methoxyphenylsulfonyl Chloride as a Fluorescent Labeling Reagent (58.6 kB)
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Copyright (c) 2009 by Fukuyama University
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| Item type | 紀要論文 / Departmental Bulletin Paper(1) | |||||
|---|---|---|---|---|---|---|
| 公開日 | 2017-01-26 | |||||
| タイトル | ||||||
| タイトル | 蛍光誘導体化試薬4-(5，6-ジメトキシ-2-フタルイミジニル)-2-メトキシフェニルスルホニルクロリドを用いる転移性骨腫瘍患者の尿中N-エチルグリシンのHPLCによる定量(発表論文抄録(2008)) | |||||
| タイトル | ||||||
| タイトル | Determination of N-Ethylglycine in Urine of Cancer Patients with Metastatic Bone Disease by HPLC Using 4-(5,6-Dimethoxy-2-phthalimidinyl)-2-methoxyphenylsulfonyl Chloride as a Fluorescent Labeling Reagent | |||||
| 言語 | en | |||||
| 言語 | ||||||
| 言語 | eng | |||||
| 資源タイプ | ||||||
| 資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
| 資源タイプ | departmental bulletin paper | |||||
| 著者 |
鶴田, 泰人
× 鶴田, 泰人× 松本, 真弥× 井上, 裕文× 宗村, 小夜香× 石津, 隆× 山野, 茂× 井口, 東郎 |
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| 著者別名 | ||||||
| 識別子Scheme | WEKO | |||||
| 識別子 | 45193 | |||||
| 姓名 | TSURUTA, Yasuto | |||||
| 著者別名 | ||||||
| 識別子Scheme | WEKO | |||||
| 識別子 | 45194 | |||||
| 姓名 | MATSUMOTO, Maya | |||||
| 著者別名 | ||||||
| 識別子Scheme | WEKO | |||||
| 識別子 | 45195 | |||||
| 姓名 | INOUE, Hirofumi | |||||
| 著者別名 | ||||||
| 識別子Scheme | WEKO | |||||
| 識別子 | 45196 | |||||
| 姓名 | MUNEMURA, Sayaka | |||||
| 著者別名 | ||||||
| 識別子Scheme | WEKO | |||||
| 識別子 | 45197 | |||||
| 姓名 | YAMANO, Shigeru | |||||
| 著者別名 | ||||||
| 識別子Scheme | WEKO | |||||
| 識別子 | 45198 | |||||
| 姓名 | IGUCHI, Haruo | |||||
| 抄録 | ||||||
| 内容記述タイプ | Abstract | |||||
| 内容記述 | A simple and highly sensitive HPLC for the determination of <i>N</i>-ethylglycine in urine was developed. The labeling reaction of <i>N</i>-ethylglycine with 4-(5,6-dimethoxy-2-phthalimidinyl)-2-methoxyphenylsulfonyl chloride was carried out at 70°C for 15 min at pH 9.0. The fluorescent derivative was separated on a reversed-phase column and detected at excitation and emission wavelengths of 320 and 400 nm, respectively. The detection limit of <i>N</i>-ethylglycine was 15 fmol (<i>S/N</i> = 3). The recovery of <i>N</i>-ethylglycine added to urine was 101.9%. The concentration of <i>N</i>-ethylglycine in urine of cancer patients with metastatic bone disease was 11.3 ± 22.0 nmol/mg creatinine, and that of normal subject was 0.4 ± 0.4 nmol/mg creatinine. | |||||
| 内容記述 | ||||||
| 内容記述タイプ | Other | |||||
| 内容記述 | A simple and highly sensitive HPLC for the determination of <i>N</i>-ethylglycine in urine was developed. The labeling reaction of <i>N</i>-ethylglycine with 4-(5,6-dimethoxy-2-phthalimidinyl)-2-methoxyphenylsulfonyl chloride was carried out at 70°C for 15 min at pH 9.0. The fluorescent derivative was separated on a reversed-phase column and detected at excitation and emission wavelengths of 320 and 400 nm, respectively. The detection limit of <i>N</i>-ethylglycine was 15 fmol (<i>S/N</i> = 3). The recovery of <i>N</i>-ethylglycine added to urine was 101.9%. The concentration of <i>N</i>-ethylglycine in urine of cancer patients with metastatic bone disease was 11.3 ± 22.0 nmol/mg creatinine, and that of normal subject was 0.4 ± 0.4 nmol/mg creatinine. | |||||
| 書誌情報 |
福山大学薬学部研究年報 en : Annual report of the Faculty of Pharmacy & Pharmaceutical Sciences, Fukuyama University 号 27, p. 37-37, 発行日 2009-12-25 |
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| 出版者 | ||||||
| 出版者 | 福山大学薬学部 | |||||
| ISSN | ||||||
| 収録物識別子タイプ | ISSN | |||||
| 収録物識別子 | 0288-724X | |||||
| 書誌レコードID | ||||||
| 収録物識別子タイプ | NCID | |||||
| 収録物識別子 | AN10064550 | |||||
