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ガロカテキン-3-O-ガレート・カフェイン錯体の立体化学構造と分子間相互作用(発表論文抄録(2011))
https://fukuyama-u.repo.nii.ac.jp/records/8810
https://fukuyama-u.repo.nii.ac.jp/records/8810813b6886-1364-4dcc-8de7-a4dfbb78fc7a
名前 / ファイル | ライセンス | アクション |
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堤広之(発表論文抄録(2011)) (93.6 kB)
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Copyright (c) 2012 by Fukuyama University
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Item type | 紀要論文 / Departmental Bulletin Paper(1) | |||||
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公開日 | 2017-12-22 | |||||
タイトル | ||||||
タイトル | ガロカテキン-3-O-ガレート・カフェイン錯体の立体化学構造と分子間相互作用(発表論文抄録(2011)) | |||||
タイトル | ||||||
言語 | en | |||||
タイトル | Stereochemical Structure and Intermolecular Interaction of Complexes of (-)-Gallocatechin-3-O-gallate and Caffeine | |||||
言語 | ||||||
言語 | jpn | |||||
キーワード | ||||||
言語 | en | |||||
主題Scheme | Other | |||||
主題 | (−)-gallocatechin-3-O-gallate | |||||
キーワード | ||||||
言語 | en | |||||
主題Scheme | Other | |||||
主題 | caffeine | |||||
キーワード | ||||||
言語 | en | |||||
主題Scheme | Other | |||||
主題 | X-ray crystallographic analysis | |||||
キーワード | ||||||
言語 | en | |||||
主題Scheme | Other | |||||
主題 | intermolecular interaction | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | departmental bulletin paper | |||||
著者 |
Tsutsumi, Hiroyuki
× Tsutsumi, Hiroyuki× Sato, Takashi× Ishizu, Takashi |
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著者別名 | ||||||
識別子Scheme | WEKO | |||||
識別子 | 45308 | |||||
識別子Scheme | CiNii ID | |||||
識別子URI | http://ci.nii.ac.jp/nrid/9000243751410 | |||||
識別子 | 9000243751410 | |||||
姓名 | 堤, 広之 | |||||
著者別名 | ||||||
識別子Scheme | WEKO | |||||
識別子 | 45311 | |||||
姓名 | 佐藤, 隆 | |||||
著者別名 | ||||||
識別子Scheme | WEKO | |||||
識別子 | 45110 | |||||
識別子Scheme | CiNii ID | |||||
識別子URI | http://ci.nii.ac.jp/nrid/9000005188259 | |||||
識別子 | 9000005188259 | |||||
姓名 | 石津, 隆 | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | A suspension containing an equimolecular amount of (−)-gallocatechin-3-O-gallate (GCg) and caffeine in water was heated at 90 °C for 30 min to give a 1 : 2 complex of GCg and caffeine. X-Ray crystallographic analysis of crystal of the 1 : 2 complex showed that π–π interactions formed between the A, B′ rings of GCg and the two six-membered rings of caffeine. Whereas, the same suspension was heated at 90 °C for 30 s to give a sticky substance, which contained GCg, caffeine, and water at a molar ratio of 1 : 1 : 22 based on measurement of the integral volume of 1H-NMR signals. The sticky substance crystallized slowly to give a 2 : 2 complex of GCg and caffeine. X-Ray crystallographic analysis of crystal of the 2 : 2 complex showed that the A and C rings of GCg moieties faced each other, and face-to-face π–π interactions formed between the B ring of GCg and caffeine, the B′ ring of GCg and caffeine. | |||||
内容記述 | ||||||
内容記述タイプ | Other | |||||
内容記述 | A suspension containing an equimolecular amount of (−)-gallocatechin-3-O-gallate (GCg) and caffeine in water was heated at 90 °C for 30 min to give a 1 : 2 complex of GCg and caffeine. X-Ray crystallographic analysis of crystal of the 1 : 2 complex showed that π–π interactions formed between the A, B′ rings of GCg and the two six-membered rings of caffeine. Whereas, the same suspension was heated at 90 °C for 30 s to give a sticky substance, which contained GCg, caffeine, and water at a molar ratio of 1 : 1 : 22 based on measurement of the integral volume of 1H-NMR signals. The sticky substance crystallized slowly to give a 2 : 2 complex of GCg and caffeine. X-Ray crystallographic analysis of crystal of the 2 : 2 complex showed that the A and C rings of GCg moieties faced each other, and face-to-face π–π interactions formed between the B ring of GCg and caffeine, the B′ ring of GCg and caffeine. | |||||
書誌情報 |
福山大学薬学部研究年報 en : Annual report of the Faculty of Pharmacy & Pharmaceutical Sciences, Fukuyama University 号 30, p. 5-5, 発行日 2012-12-25 |
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出版者 | ||||||
出版者 | 福山大学薬学部 | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 0288-724X | |||||
書誌レコードID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AN10064550 |